Bis(diphenylphosphinophenyl)ether palladium (II) dichloride
Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II)
CAS: 205319-06-8
Molecular Formula: C36H28Cl2OP2Pd
Bis(diphenylphosphinophenyl)ether palladium (II) dichloride - Names and Identifiers
| Name | Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) |
| Synonyms | Pd-117 bis(diphenylphosphinophenyl)etherpalladium(II)... Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) Bis(diphenylphosphinophenyl)ether palladium (II) dichloride Dichloro[bis(2-(diphenylphosphino)phenyl)ether]palladium(II) cis-[Bis[2-(diphenylphosphino)phenyl] ether]dichloropalladium Bis(diphenylphosphinophenyl)ether palladium (II) dichloride |
| CAS | 205319-06-8 |
| InChI | InChI=1/C36H28OP2.2ClH.Pd/c1-5-17-29(18-6-1)38(30-19-7-2-8-20-30)35-27-15-13-25-33(35)37-34-26-14-16-28-36(34)39(31-21-9-3-10-22-31)32-23-11-4-12-24-32;;;/h1-28H;2*1H;/q;;;+2/p-2 |
Bis(diphenylphosphinophenyl)ether palladium (II) dichloride - Physico-chemical Properties
| Molecular Formula | C36H28Cl2OP2Pd |
| Molar Mass | 717.9 |
| Melting Point | 243-250°C |
| Boling Point | 608.2°C at 760 mmHg |
| Flash Point | 404.9°C |
| Water Solubility | Insoluble in water. |
| Vapor Presure | 4.35E-14mmHg at 25°C |
| Appearance | Powder |
| Color | yellow |
| Storage Condition | 2-8°C |
| MDL | MFCD09953446 |
Bis(diphenylphosphinophenyl)ether palladium (II) dichloride - Risk and Safety
| Risk Codes | 36/37/38 - Irritating to eyes, respiratory system and skin. |
| Safety Description | S26 - In case of contact with eyes, rinse immediately with plenty of water and seek medical advice. S37 - Wear suitable gloves. |
| WGK Germany | 3 |
| TSCA | No |
Bis(diphenylphosphinophenyl)ether palladium (II) dichloride - Introduction
Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II), chemical formula [PdCl2(Ph2P(CH2)nPPh2)](n = 1-4), is an organometallic compound. It is usually powdered and insoluble in common organic solvents.
Nature:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is a complex soluble in alcohols and chlorinated hydrocarbons.
2. It is relatively stable in the air and can be stored for a long time in a dry environment.
3. It is a liquid crystal material that can be used in display manufacturing.
Use:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is commonly used as a catalyst and has important applications in organic synthesis. It can catalyze the polymerization of olefins, aromatization and hydrogenation of alkynes.
2. It can also be used as a photosensitizer for the preparation of photosensitive materials.
Method:
The preparation of Dichloro[bis(diphenyl phosphinophenyl)ether]palladium(II) generally requires the use of synthetic organometallic chemistry methods, usually in the presence of palladium chloride (II), synthesis of phenylphosphine and phenyl ether by heating with dichloromethane or carbon tetrachloride.
Safety Information:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is irritating to the skin and eyes, and protective gloves and eye protection are required during operation.
2. In the process of operation to avoid contact with the skin and inhalation of dust.
3. Waste recycling as far as possible or according to local regulations.
Nature:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is a complex soluble in alcohols and chlorinated hydrocarbons.
2. It is relatively stable in the air and can be stored for a long time in a dry environment.
3. It is a liquid crystal material that can be used in display manufacturing.
Use:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is commonly used as a catalyst and has important applications in organic synthesis. It can catalyze the polymerization of olefins, aromatization and hydrogenation of alkynes.
2. It can also be used as a photosensitizer for the preparation of photosensitive materials.
Method:
The preparation of Dichloro[bis(diphenyl phosphinophenyl)ether]palladium(II) generally requires the use of synthetic organometallic chemistry methods, usually in the presence of palladium chloride (II), synthesis of phenylphosphine and phenyl ether by heating with dichloromethane or carbon tetrachloride.
Safety Information:
1. Dichloro[bis(diphenylphosphinophenyl)ether]palladium(II) is irritating to the skin and eyes, and protective gloves and eye protection are required during operation.
2. In the process of operation to avoid contact with the skin and inhalation of dust.
3. Waste recycling as far as possible or according to local regulations.
Last Update：2024-04-10 22:29:15
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